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Fig 1.

Experimental procedure flow.

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Fig 1 Expand

Fig 2.

Mineral fractions of rock samples.

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Fig 2 Expand

Fig 3.

T2 spectra distribution of samples.

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Fig 3 Expand

Fig 4.

Schematic diagram of test stress unloading path.

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Fig 4 Expand

Fig 5.

Images of SEM after unloading disturbance.

Note: (a) The unloading amplitude is 10MPa; (b) The unloading amplitude is 20MPa; (c) The unloading amplitude is 30MPa; (d) The unloading amplitude is 40MPa; (e) The unloading amplitude is 50MPa; (f) The unloading amplitude is 60MPa.

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Fig 5 Expand

Fig 6.

Images of SEM after binary processing.

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Fig 7.

Image digitization process.

Note: (a) Continuous image that has been projected onto the sensor array; (b) Results of image sampling and quantization.

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Table 1.

Porosity and void ratio of each binary image.

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Table 1 Expand

Table 2.

Microcosmic pores parameters calculation results.

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Table 2 Expand

Table 3.

Percentage of different dmax/dmin.

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Table 3 Expand

Table 4.

Statistical parameters of T2 energy spectrum under different unloading amplitudes.

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Table 4 Expand

Fig 8.

Image details.

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Fig 8 Expand

Fig 9.

Statistics of pore structure parameters in selected areas.

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Fig 10.

Aperture parameters.

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Fig 11.

Number percentage of pores with different dmax/dmin ratios.

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Fig 12.

Area percentage of pores with different dmax/dmin ratios.

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Fig 13.

Shale T2 energy spectrum with different unloading amplitudes.

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Fig 13 Expand

Fig 14.

T2 energy spectrum area growth rate after pores after different unloading amplitudes.

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Fig 14 Expand

Fig 15.

Proportion of various unloading amplitudes.

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Fig 15 Expand

Fig 16.

Percent stacking chart of micropore, mesopore, and macropore spectrum area.

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Fig 17.

T2 spectrum distribution in the saturated state and after centrifugation.

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Fig 17 Expand

Table 5.

Pore change of rock samples with unloading amplitudes.

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Table 5 Expand

Fig 18.

Variation of shale void ratio and expansion rate after unloading disturbance.

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Fig 18 Expand

Fig 19.

Shale triaxial compression test after unloading disturbance.

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Fig 20.

Variation of shear strength and elastic modulus with different unloading amplitudes.

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Fig 20 Expand

Table 6.

Porosity and expansion rate under unloading disturbance after returning to formation stress.

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Table 6 Expand

Fig 21.

Changing law of rock expansion rate with different unloading amplitude.

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Fig 21 Expand

Table 7.

Rock shear strength limit value and damage variable after unloading disturbance.

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Table 7 Expand

Table 8.

Model parameters.

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Table 8 Expand

Fig 22.

Variation law of damage variables after unloading disturbance.

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Fig 22 Expand