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Fig 1.

A. A costum-made metal cone with a wide opening and space for a wide-mouth vial containing the sample. B. Example of the experimental setup for training and testing environment, with the positive sample positioned on the 4th cone.

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Fig 2.

Experimental design of training and testing sessions.

A. Training session: Dogs were trained during 1–4 days with three lines of motivation of followed by a simple blinded lines with the tested concentration. When the dog successfully passes the level of concentration during testing (success in more than 75% of the lines), he was tested in a double-blind situation (B). B. Testing session: The testing session consists of three lines of motivation, two or three lines of simple blind tests, then four lines of double-blind tests. In the preliminary single-blinded phase, we required dogs to correctly complete two trials before advancing to the double-blinded phase. If a dog succeeded in only one out of the first two trials, a third trial was conducted to provide an additional opportunity for qualification.

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Fig 3.

Performance of two dogs relative to concentration levels.

On the y-axis are the performances of the dogs in %, by concentration. The concentrations are indicated on the x-axis The success threshold is set at 75%.

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Table 1.

Coding scheme for behaviours associated with marking.

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Table 2.

General overview of the results, including the total number of trials and double-blinded conditions. Results are presented as absolute values, with square brackets indicating the range (minimum to maximum) and percentages shown in parentheses.

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Table 3.

Dogs’ behaviour and performance linked to sample age during double-blinded tests. Percentages are shown in parenthesis.

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Table 4.

Description of position of negative marked samples in urine, in double-blinded settings. Percentages are shown in parenthesis.

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