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Table 1.

B1, B2, B6, and B8 vitamins available commercial formulations and required oral unidose formulas.

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Table 2.

Compounding formulas for 300 hard gelatin vitamin capsules.

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Table 2 Expand

Table 3.

HPLC stability-indicating dosing methods, general parameters.

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Table 3 Expand

Table 4.

Vitamin capsules treatment before HPLC-UV analysis.

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Table 5.

Thiamine, riboflavine, pyridoxine and biotine method validation.

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Table 6.

Thiamine chlorhydrate forced degradation.

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Table 7.

Riboflavine forced degradation.

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Table 7 Expand

Table 8.

Pyridoxine chlorhydrate forced degradation.

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Table 9.

Biotin forced degradation.

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Table 10.

System Suitability Test for vitamin stability-indicating dosing methods.

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Table 11.

Vitamin hard gelatin capsules, batches released and rejected since implementation.

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Fig 1.

Content variation of vitamin capsules stored at ambient temperature (25 °C/ 60% RH) over time.

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Fig 2.

Content variation of thiamine hydrochloride 50 mg capsules from protocol 2 stored at ambient temperature (25 °C/ 60% RH) over time.

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