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Fig 1.

Outline of the research protocol adopted for this study.

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Fig 1 Expand

Fig 2.

Pictorial representation of (a) non-tire automotive rubber particles, (b) PPO, and (c) sulfur.

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Table 1.

Physical characteristics of base binder.

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Table 1 Expand

Fig 3.

Schematic illustration for the formulation of composite asphalt binder.

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Table 2.

Nomenclature and compositional information of studied asphalt formulations.

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Table 2 Expand

Fig 4.

Schematics for rubber extraction test.

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Table 3.

Specifics of separation indices (SIs).

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Table 3 Expand

Fig 5.

Softening point difference results after (a) 48 h and (b) 96 h of thermal storage.

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Fig 6.

SI based on rotational viscosity after (a) 48 h and (b) 96 h of thermal storage.

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Fig 7.

SI based on G*/sin δ after (a) 48 h and (b) 96 h of thermal storage.

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Fig 8.

SI based on MSCR Jnr after (a) 48 h and (b) 96 h of thermal storage.

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Fig 9.

FTIR spectra of top and bottom parts of (a) binder R and (b) binder RP6p.

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Fig 10.

Chemical separation index (SIFTIR) after (a) 48 h and (b) 96 h of thermal storage.

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Fig 11.

Chemical separation index (SIFTIR) as a function of (a) SPD and (b) SIG*/sin δ.

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Fig 12.

AFM micrographs after 48 h of thermal storage of binders: (a) R-top, (b) R-bottom, (c) RP6-top, (d) RP6-bottom, (e) RP6p-top, (f) RP6p-bottom; and after 98 h of thermal storage of binders: (g) R-top, (h) R-bottom, (i) RP6-top, (j) RP6-bottom, (k) RP6p-top, (l) RP6p-bottom.

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Fig 13.

SIRET results from rubber extraction test after (a) 48 h and (b) 96 h of thermal storage.

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Fig 14.

SIRET as a function of (a) SPD and (b) SIG*/sin δ.

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Fig 14 Expand