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Fig 1.

FT-IR spectra of pristine FDU-12, FDU-12-MA, FDU-12-TA, pristine PMMA, FDU-12-MA/PMMA, pristine NY6, and FDU-12-TA/NY6.

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Fig 1 Expand

Fig 2.

FE-SEM images of pristine FDU-12, FDU-12-MA, FDU-12-TA, FDU-12-MA/PMMA, and FDU-12-TA/NY6 at three magnifications.

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Fig 2 Expand

Fig 3.

TEM images of pristine FDU-12.

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Fig 3 Expand

Fig 4.

N2 adsorption/desorption isotherms of (a) pristine FDU-12, (b) FDU-12-MA, (c) FDU-12-TA, and (d) the BJH pore size distribution curves of the samples.

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Fig 4 Expand

Table 1.

Textural properties of the synthesized pristine FDU-12, FDU-12-MA, and FDU-12-TA.

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Table 1 Expand

Fig 5.

The effect of (a) pH, (b) adsorbent amount, and (c) contact time on adsorption of Pb(II) by the prepared adsorbents.

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Fig 5 Expand

Fig 6.

The kinetic adsorption models of (a) pseudo-first-order, (b) pseudo-second-order, (c) Elovich, (d) intra-particle diffusion; (e) the equilibrium isotherm and the isotherm models of (f) Langmuir, (g) Freundlich, and (h) Dubinin–Radushkevich for the adsorption of Pb(II) onto FDU-12-MA/PMMA and FDU-12-TA/NY6.

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Fig 6 Expand

Table 2.

The parameters obtained by kinetic models for the adsorption of Pb(II) onto FDU-12-MA/PMMA and FDU-12-TA/NY6.

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Table 2 Expand

Table 3.

The parameters obtained by isotherm models for the adsorption of Pb(II) onto FDU-12-MA/PMMA and FDU-12-TA/NY6.

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Table 3 Expand

Table 4.

Comparison of the adsorption capacity of FDU-12-MA/PMMA and FDU-12-TA/NY6 toward Pb(II) ions with other adsorbents.

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Table 4 Expand

Fig 7.

The calculated values of RL.

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Fig 7 Expand