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Fig 1.

Schematic illustration of the experimental setup.

A three-electrode setup and sampling port were incorporated in four-neck round-bottom flasks. In one-chamber reactors, working and counter electrode are located in one compartment. Therefore, Geobacter spp. enrichment biofilms can consume cathodically produced hydrogen. In two-chamber reactors, a counter electrode chamber with a fixed cation exchange membrane is introduced minimizing crossover of cathodically produced hydrogen. All reactors were sampled at the beginning as well as at the end of a batch cycle and every 6 h during a batch cycle for obtaining total (CEt) and incremental coulombic efficiencies (CEi), respectively.

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Fig 1 Expand

Table 1.

List of total coulombic efficiencies derived from studies cultivating Geobacter sulfurreducens and Geobacter spp. enrichment biofilms in one- and two-chamber reactors.

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Table 1 Expand

Table 2.

List of studies that applied Michaelis-Menten kinetics to Geobacter sulfurreducens and Geobacter spp. enrichment biofilms and determined KM and vmax values.

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Table 2 Expand

Fig 2.

Temporal progressions of current density (j), acetate concentration (CAc), and incremental coulombic efficiency (CEi) of two-chamber reactors.

R1-3 represent experimental replicates. Open circles indicate sampling events. Vertical dashed line indicates beginning of 2nd batch cycle after medium exchange.

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Fig 2 Expand

Fig 3.

Temporal progressions of current density (j), acetate concentration (CAc), and incremental coulombic efficiency (CEi) of one-chamber reactors.

R4-6 represent experimental replicates. Open circles indicate sampling events. Vertical dashed line indicates beginning of 2nd batch cycle after medium exchange.

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Fig 3 Expand

Table 3.

List of total coulombic efficiencies (CEt) determined in this study.

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Table 3 Expand

Fig 4.

Dot plots of (A) maximum substrate uptake rate (vmax,i) and (B) half-saturation concentration (KM,i) based on either acetate uptake (closed circles) or current production (open circles) derived from Michaelis-Menten kinetics regression analysis of two- and one-chamber reactors. As the prolonged current decrease and slower acetate uptake of R3 impaired application of Michaelis-Menten kinetics, respective results were omitted from this data comparison. bc: batch cycle.

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Fig 4 Expand