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Table 1.

Demographic data for subjects providing primary human airway epithelial cells.

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Table 1 Expand

Fig 1.

Effect of IFNγ in the presence and absence of TNFα on the release of CXCL9, CXCL10 and CXCL11 from BEAS-2B and primary human airway epithelial cells.

BEAS-2B cells, n = 11 (open bars, panels a, c and e) or human primary airway epithelial cells from non-smokers (n = 4) (closed bars), smokers (n = 5) (horizontal lines) or patients with COPD (n = 7) (hatched bars) (panels b, d and f) were incubated for 20h in the absence or presence of IFNγ (10ng/ml) or IFNγ + TNFα (10ng/ml). Media was harvested and the concentrations of CXCL9 (panels a and b), CXCL10 (panels c and d) and CXCL11 (panels e and f) were measured by ELISA. Data are presented as mean ± SEM, where * represents p<0.05, **p<0.01 and ***p<0.001.

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Fig 2.

Effect of JAK inhibitors, PF956980 and PF1367550 and dexamethasone on IFNγ and IFNγ + TNFα-stimulated release of CXCL9, CXCL10 and CXCL11 from BEAS-2B cells.

BEAS-2B cells were pre-treated and incubated for 1h with either PF956980 (○), PF1367550 (●), or dexamethasone (▲) followed by stimulation for 20h with IFNγ (10ng/ml) (panels a-c) or IFNγ + TNFα (10ng/ml) (panels d-f). Media was harvested and the concentrations of CXCL9 (panels a and d), CXCL10 (panels b and e) and CXCL11 (panels c and f) were measured by ELISA. Data are presented as mean±SEM, n = 7–8.

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Fig 2 Expand

Table 2.

Selectivity of PF1367550.

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Table 2 Expand

Table 3.

IC50 values for PF956980 and PF1367550 on IFNγ and IFNγ+TNFα-stimulated release of CXCL9, CXCL10 and CXCL11 from BEAS-2B cells.

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Table 3 Expand

Fig 3.

Effect of JAK inhibitors, PF956980 and PF1367550 and dexamethasone on IFNγ and IFNγ+TNFα-stimulated release of CXCL9, CXCL10 and CXCL11 from human primary airway epithelial cells.

Human primary airway epithelial cells were pre-treated for 1h with either PF956980 (○), PF1367550 (●), or dexamethasone (▲) followed by stimulation for 20h with IFNγ (10 ng/ml) (panels a-c) or IFNγ + TNFα (10 ng/ml) (panels d-f). Media was harvested and the concentrations of CXCL9 (panels a and d), CXCL10 (panels b and e) and CXCL11 (panels c and f) were measured by ELISA. Data are presented as mean ± SEM, n = 10–13.

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Fig 3 Expand

Table 4.

IC50 values for PF956980 and PF1367550 on IFNγ and IFNγ+TNFα-stimulated release of CXCL9, CXCL10 and CXCL11 from human primary airway epithelial cells from non-smokers, smokers and COPD patients.

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Table 4 Expand

Table 5.

IC50 values for PF956980 and PF1367550 on IFNγ and IFNγ+TNFα-stimulated release of CXCR3 chemokinesCXCL9, CXCL10 and CXCL11 from human primary airway epithelial cells.

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Table 5 Expand

Fig 4.

Effect of JAK inhibitors, PF956980 and PF1367550 on IFNγ and IFNγ + TNFα-stimulated phosphorylation of STAT-1 in BEAS-2B cells.

BEAS-2B cells were pre-treated for 1h with either PF956980 or PF1367550 followed by stimulation for 10 min with IFNγ (10ng/ml) (○) or IFNγ + TNFα (●). Cells were harvested and western blots performed for phosphorylated STAT-1 and total STAT-1 and quantified by densitometry. Data are representative of n = 4 independent experiments (panels a and c) and presented as mean±SEM, n = 4 (panels b and d).

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Fig 4 Expand

Fig 5.

Effect of JAK inhibitors, PF956980 and PF1367550 on IFNγ and IFNγ + TNFα-stimulated phosphorylation of STAT-1 in human primary airway epithelial cells.

Human primary airway epithelial cells were pre-treated for 1h with either 1μM PF956980 (PF956) or 1μM PF1367550 (PF136) followed by stimulation for 10 min with either IFNγ (10ng/ml) or IFNγ + TNFα. Cells were harvested and western blots performed for phosphorylated STAT-1 and total STAT-1 and quantified by densitometry. Data are representative of n = 4 independent experiments (panel a) and presented as mean ± SEM, n = 4 (panel b).

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Fig 5 Expand

Fig 6.

Effect of JAK inhibitors, PF956980 and PF1367550 on IFNγ and IFNγ + TNFα-stimulated DNA binding of STAT-1 and STAT-3 in BEAS-2B cells.

BEAS-2B cells were pre-treated with either PF956980 (PF956) or PF1367550 (PF136) for 1h followed by stimulation with IFNγ (10ng/ml) or IFNγ + TNFα. After 1 h, nuclear extracts of the cells were prepared and TransAM assays for STAT-1 (panel a) and STAT-3 (panel b) were performed. Data are presented as fold change from baseline ± SEM; n = 4.

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Fig 7.

Effect of JAK inhibitors, PF956980 and PF1367550 on IFNγ and IFNγ + TNFα-stimulated expression of CXCL9, CXCL10, and CXCL11.

BEAS-2B cells were pre-treated with either PF956980 (checked bars), PF1367550 (hashed bars) or dexamethasone (10-6M white bar) for 1h followed by stimulation with IFNγ (10ng/ml) or IFNγ + TNFα for 6 h. Gene expression of CXCL9 (panels a and b), CXCL10 (panels c and d) and CXCL11 (panels e and f) were quantified by Taqman RT-PCR. Data are presented as fold change form stimulus ± SEM; n = 3 where 1 indicates the level of mRNA induced by IFNγ or IFNγ + TNFα in the absence of inhibitors.

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Fig 7 Expand