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Figure 1.

Effect of vorinostat on IGF-I-mediated signal transduction.

Ishikawa and USPC-2 cells were treated for 24 h with vorinostat (or left untreated) and/or IGF-I during the last 10 min of the incubation period. Whole-cell lysates (100 µg) were resolved on SDS-PAGE and immunoblotted with antibodies against pIGF-IR, TIGF-IR, pAKT, TAKT, pERK1/2, TERK1/2, p21, and actin. The figure shows the result of a typical experiment, repeated three times with similar results. IGF-IR phosphorylation in USPC-2 cells was significantly lower than in Ishikawa cells and was detected by Western blot analysis only after longer exposure times of blots to X-ray film. Therefore, this experiment does not allow comparison between both cell lines in terms of levels of expression or phosphorylation.

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Figure 2.

Effect of vorinostat on apoptosis and acetyl-histone H3.

Western blot analysis of PARP (A) on Ishikawa and USPC-2 cells and caspase 3 (B), Bcl2 (C) and caspase 8 (D) on USPC-2 cells. Cells were treated with vorinostat for 24 h in the absence or presence of IGF-I. After incubation, cell lysates were prepared and electrophoresed (100 µg for Bcl2 or 70 µg for caspases 3 and 8). Caspase 3 expression in USPC-2 cells was detected after a long exposure time of blots to X-ray film. Results are representative of three independent experiments.

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Figure 3.

Effect of vorinostat on p53 and pTEN expression.

Ishikawa and USPC-2 cells were treated for 24 h with vorinostat (or left untreated) and/or IGF-I. Whole-cell lysates (100 µg) were resolved on SDS-PAGE and immunoblotted with antibodies against p53, pTEN, acetyl-histone H3 and actin. Western blot analysis revealed that basal p53 levels were much lower in USPC-2 than in Ishikawa cells and were detected after long exposure times. Results represent a typical experiment out of three independent experiments.

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Figure 4.

Regulation of IGF-IR promoter activity by vorinostat in endometrial cancer cells.

Ishikawa and USPC-2 cells were transiently transfected with an IGF-IR promoter-luciferase reporter plasmid, p(−476/+640)LUC, which contains most of the proximal region of the IGF-IR promoter, and a ß-galactosidase vector. Promoter activity is expressed as luciferase values normalized for ß-galactosidase. A value of 100% was given to the promoter activity in the absence of vorinostat. Results are mean ± S.E.M. (three independent experiments); p*<0.01 versus untreated cells.

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Figure 5.

Effect of vorinostat on endometrial cancer cells proliferation.

Cells were plated in 24-well plates at a density of 2×104 cells/well for Ishikawa (A) and 3×104 cells/well for USPC-2 (B). The bars represent the mean ± S.E.M. of three independent experiments, performed each in triplicate; * p<0.05 versus untreated cells.

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Table 1.

Effect of vorinostat on the cell cycle in endometrial cancer cells.

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Table 1 Expand

Figure 6.

Effect of vorinostat on the mTor and Ampk signaling pathway in endometrial cancer cells.

Ishikawa and USPC-2 cells were treated with vorinostat and/or IGF-I, and cell lysates (100 µg) were prepared after 24 h. Western blot analysis was performed with antibodies against pmTor, T-mTor, p-Ampk, T-Ampk, p21, cyclin D1, PI3K and actin. The figure shows the results of a typical experiment, repeated three times with similar results.

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Figure 7.

Colony formation in soft agar.

A total of 1.5×104 Ishikawa cells and 1.2×104 USPC-1 cells were seeded on 6-well plates in soft agar. The formed colonies were photographed at a magnification of 40× and 200× (A) and colonies with diameters greater than 3 mm were counted (B) at day 22. The bars represent the mean ± S.E.M. of three independent wells; * p<0.05 versus untreated cells.

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Figure 8.

Effect of vorinostat on wound healing assays in endometrial cancer cells.

Wounds were made on monolayers of Ishikawa (A) and USPC-2 (B) cells grown to 100% confluence. Untreated (control) cells or cells treated with vorinostat and/or IGF-I were photographed just after scratch (time 0), and after 48 h and 72 h. Results presented here are representative of triplicate independent samples of each cell line.

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Figure 9.

Effect of vorinostat and/or antibody MK-0646 on apoptosis and IGF-IR protein levels.

Ishikawa and USPC-2 cells were treated with vorinostat for 24 h, separately and in combination with MK-0646, in the presence or absence of IGF-I. Whole-cell lysates (70 µg for caspase 9 and 100 µg for total IGF-IR and p21 proteins detection) were resolved by SDS-PAGE and immunoblotted with antibodies against T-IGF-IR and p21 (A) and caspase 9 (B). The figure shows the results of a typical experiment, repeated twice with similar results.

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