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Table 1.

Clostridia strains used in this study.

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Figure 1.

PFGE experiments showing the presence of an extrachromosomal mega-sized DNA band of > 600 kb in the undigested genomic DNA preparations from 10 neurotoxigenic C. butyricum type E strains: ISS-145/1 (lane 2); ISS-20 (lane 3); ISS-21 (lane 4); ISS-109 (lane 5); ISS-86 (lane 6); ISS-190 (lane 7); KZ-1886 (lane 8); KZ-1890 (lane 9); LCL-063 (lane 10); LCL-155 (lane 11).

An additional extrachromosomal smaller band is evident in the DNA preparations from neurotoxigenic type E strains ISS-145/1, ISS-20, ISS-21, ISS-109, ISS-86, ISS-190 (lanes 2–7), and KZ-1890 (lane 9). Lane 1, undigested genomic DNA from non-neurotoxigenic C. butyricum strain ATCC 19398. S.e., XbaI-digested genomic DNA fragments of Salmonella enterica serotype Braenderup strain H9812 (ref. 35). S.c., Saccharomyces cerevisiae chromosomal DNA size marker (Biorad). PFGE conditions: 5–60 s pulse at 6 V/cm for 18 h (1a), and 50–90 s pulse at 6 V/cm for 20 h (1b). At the different PFGE conditions applied, the apparent sizes of the extrachromosomal mega-sized DNA bands (lanes 2–11) did not change in relation to the linear bands of the molecular size standards, consistent with the behaviour expected for linear DNA molecules. The mega-band sizes were estimated as follows (Figure 1b): >610 kb for strains ISS-20, ISS-21, ISS-109, ISS-145/1 (lanes 2–5); ∼825kb for strains ISS-86, ISS-190, LCL-063 and LCL-155 (lanes 6, 7, 10 and 11); and between 750 and 785 kb for strains KZ-1886 and KZ-1890 (lanes 8, 9). Migration of the extrachromosomal smaller DNA bands relative to the linear DNA markers was inconsistent (lanes 2–7 and lane 9 of Figures 1a and 1b), consistent with the behavior expected for circular super-coiled DNA molecules: as a consequence, the actual size of the extrachromosomal smaller bands of strains ISS-145/1, ISS-20, ISS-21, ISS-109, ISS-86, ISS-190 and KZ-1890 could not be determined.

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Figure 2.

PFGE analysis of genomic DNA of six neurotoxigenic C. butyricum type E strains representative of the different megaplasmids sizes: ISS-109 (lanes 1 and 2); ISS-190 (lanes 3 and 4); KZ-1886 (lanes 5 and 6); KZ-1890 (lanes 7 and 8); LCL-063 (lanes 9 and 10); LCL-155 (lanes 11 and 12).

S.e., XbaI-digested genomic DNA fragments of Salmonella enterica serotype Braenderup strain H9812 (ref. 35). PFGE conditions: 5–60 s pulse at 6 V/cm for 18 h. − and + indicate absence and presence of treatment with ATP-dependent exonuclease, respectively. The megaplasmid bands disappeared after treatment with the ATP-dependent nuclease, an enzyme that selectively digests linear DNA molecules, indicating that all megaplasmids had a linear structure (lanes 2, 4, 6, 8, 10, 12). The smaller plasmids of strains ISS-109 (lanes 1 and 2) and ISS-190 (lanes 3 and 4) were not susceptible to the ATP-dependent nuclease treatment, indicating that they had a circular structure. The ∼167 kb band of strain KZ-1890 disappeared after the ATP-dependent nuclease treatment (lanes 7 and 8), indicating that it was a linear DNA molecule; however, the same plasmid of strain KZ-1890 showed inconsistent PFGE migration typical of supercoiled DNA (lane 9 of Figures 1a and 1b). Hence, the smaller plasmid of strain KZ-1890 can exist in both linear and supercoiled forms, consistent with the behavior expected for circular DNA.

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Figure 3.

PFGE of undigested genomic DNA of non-neurotoxigenic C. butyricum strains (lanes 1–4) and C. botulinum type E strains (lanes 5–7).

Strains: UC-9035 (lane 1); UC-9041 (lane 2); GP1 (lane 3); ATCC 19398 (lane 4); CDC-5234 (lane 5); CDC-4581 (lane 6); CDC-5380 (lane 7). S.e., XbaI-digested genomic DNA fragments of Salmonella enterica serotype Braenderup strain H9812 (ref. 35). PFGE conditions: 5–60 s pulse at 6 V/cm for 18 h. Extrachromosomal bands close to the 54.7 kb band of the molecular standard (S.e.) are evident in lane 3 (non-neurotoxigenic C. butyricum strain GP1) and lane 6 (C. botulinum type E strain CDC-4581).

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Figure 4.

Clustering analysis of the PFGE profiles of the ten neurotoxigenic C. butyricum type E strains obtained by XhoI (4a) and SmaI (4b) endonucleases.

The similarity of PFGE profiles was evaluated using the Bionumerics software (version 4.0) (Applied Maths, Sint-Martens-Latem, Belgium); a similarity level of ≥ 90% was used to define PFGE groups. The 10 neurotoxigenic C. butyricum type E strains were divided in 6 PFGE groups with both endonucleases.

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Figure 5.

PFGE of undigested genomic DNA of strains ISS-145/1 (lane 1); ISS-20 (lane 2); ISS-21 (lane 3); ISS-109 (lane 4); ISS-86 (lane 5); ISS-190 (lane 6); KZ-1886 (lane 7); KZ-1890 (lane 8); LCL-063 (lane 9); LCL-155 (lane 10).

S.e., XbaI-digested genomic DNA fragments of Salmonella enterica serotype Braenderup strain H9812 (ref. 34). PFGE conditions: 5–60 s pulse at 6 V/cm for 18 h (5a). Southern hybridization with a bont/E gene probe showing that the gene probe hybridized to the chromosome bands of strains (5b). Southern hybridization with a β-lactamase gene probe showing that the gene probe hybridized to the megaplasmids of strains ISS-145/1 (lane 1); ISS-20 (lane 2); ISS-21 (lane 3); ISS-109 (lane 4); ISS-86 (lane 5); ISS-190 (lane 6); LCL-063 (lane 9); LCL-155 (lane 10) (5c).

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Figure 6.

PFGE of XhoI-digested DNA of strains ISS-145/1 (lane 1); ISS-20 (lane 2); ISS-21 (lane 3); ISS-109 (lane 4); ISS-86 (lane 5); ISS-190 (lane 6); KZ-1886 (lane 7); KZ-1890 (lane 8); LCL-063 (lane 9); LCL-155 (lane 10).

S.e., XbaI-digested genomic DNA fragments of Salmonella enterica serotype Braenderup strain H9812 (ref. 34). PFGE conditions: 4–40 s pulse at 6 V/cm for 18 h (6a). Southern hybridization with a bont/E gene probe showing that the gene probe hybridized to single restriction bands, as indicated by the black arrows (6b).

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Figure 7.

PFGE of undigested genomic DNA of strains ATCC 19398 (lane 1); ISS-145/1 (lane 2); ISS-20 (lane 3); ISS-21 (lane 4); ISS-109 (lane 5); ISS-86 (lane 6); ISS-190 (lane 7); KZ-1886 (lane 8); KZ-1890 (lane 9); LCL-063 (lane 10); LCL-155 (lane 11) (7a).

S.e., XbaI-digested genomic DNA fragments of Salmonella enterica serotype Braenderup strain H9812 (ref. 35). PFGE conditions: 5–60 s pulse at 6 V/cm for 18 h. Southern hybridization with a specific mobA gene probe showing that the gene probe hybridized to the smaller plasmids observed in lanes 2–7 (strains ISS-145/1, ISS-20, ISS-21, ISS-109, ISS-86, ISS-190) (7b).

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Table 2.

Primers used to generate the specific gene probes for the Southern blot experiments.

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