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Evaluation of mass spectrometry MS/MS spectra for the presence of isopeptide crosslinked peptides

Fig 3

Immunopurified isopeptide from MAP-rich tubulin.

Panel A shows that immunopurification on Dynabeads-Protein G-anti-isopeptide 81D1C2 yielded a single peptide eluting at 20.24 min. Panel B is the MS/MS spectrum of the immunopurified, naturally-occurring isopeptide in MAP-rich tubulin. The crosslink is between K368 of Tau and Q112 of NFH. The quadruply-charged parent ion is at 401.96 m/z.

Fig 3

doi: https://doi.org/10.1371/journal.pone.0254450.g003