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Role of the Substrate Specificity-Defining Residues of Human SIRT5 in Modulating the Structural Stability and Inhibitory Features of the Enzyme

Fig 5

Real-time Progress Curve for SIRT5-catalyzed Desuccinylation Reaction.

The time courses of the SIRT5 catalyzed reaction using the fixed concentrations of Ac-Suclys-AMC substrate and NAD+, and varying concentrations of trypsin as the coupling enzyme are shown. The dashed curves represent the time dependent increase in fluorescence at 460 nm (λex = 350 nm) due to release of 7-hydroxyl-4-methylcoumarin (AMC) from the substrate. The solid lines indicate the linear regression analysis of the data after the initial lag phases (the dashed curves).

Fig 5

doi: https://doi.org/10.1371/journal.pone.0152467.g005