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Stereochemical Control in the Still-Wittig Rearrangement Synthesis of Cyclohexyl (Z)-Alkene Inhibitors of Pin1

Fig 3

Synthesis and determination of the stereochemistry of derivative (2S,3R)-13.

Cyclic compounds 13 were synthesized. 1H NMR coupling constants (J) were used to determine the relative stereochemistry at the carbons to which Ha and Hb are attached.

Fig 3

doi: https://doi.org/10.1371/journal.pone.0139543.g003