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Determination of Olanzapine and N-desmethyl-olanzapine in Plasma Using a Reversed-Phase HPLC Coupled with Coulochemical Detection: Correlation of Olanzapine or N-desmethyl-olanzapine Concentration with Metabolic Parameters

Figure 1

Representative chromatograms.

(A) pure standard of 5 ng/ml N-desmethyl-olanzapine, 5 ng/ml olanzapine and 80 ng/ml clozapine dissolved in mobile phase without extraction; (B) pure standard of 20 ng/ml N-desmethyl-olanzapine, 20 ng/ml olanzapine and 80 ng/ml clozapine dissolved in mobile phase without extraction; (C) blank extracted plasma sample; (D) Extracted plasma sample spiked with 5 ng/ml N-desmethyl-olanzapine, 5 ng/ml olanzapine and 80 ng/ml clozapine; (E) Extracted plasma sample spiked with 20 ng/ml N-desmethyl-olanzapine, 20 ng/ml olanzapine and 80 ng/ml clozapine.

Figure 1

doi: https://doi.org/10.1371/journal.pone.0065719.g001