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An Economical Method for Production of 2H,13CH3-Threonine for Solution NMR Studies of Large Protein Complexes: Application to the 670 kDa Proteasome

Figure 2

Scheme used for the biosynthesis of U-[2H],Thr-γ2[13CH3], 6.

Enzyme name abbreviations: KHGA = 2-keto-4-hydroxyglutarate aldolase, AAT = aspartate aminotransferase, HSK = homoserine kinase, TS = threonine synthase, BCAT = branched-chain-amino-acid aminotransferase.

Figure 2

doi: https://doi.org/10.1371/journal.pone.0043725.g002