Nanogram-Scale Preparation and NMR Analysis for Mass-Limited Small Volatile Compounds

Open Access

Peer-reviewed

Research Article

Satoshi Nojima,

Current address: Shin-Etsu Chemical Co., Ltd. Tokyo, Japan

Affiliation Department of Entomology and W. M. Keck Center for Behavioral Biology, North Carolina State University, Raleigh, North Carolina, United States of America
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David J. Kiemle,

Affiliation Department of Chemistry, State University of New York-Environmental Science and Forestry, Syracuse, New York, United States of America
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Francis X. Webster,

Affiliation Department of Chemistry, State University of New York-Environmental Science and Forestry, Syracuse, New York, United States of America
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Charles S. Apperson,

Affiliation Department of Entomology and W. M. Keck Center for Behavioral Biology, North Carolina State University, Raleigh, North Carolina, United States of America
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Coby Schal

* E-mail: coby_schal@ncsu.edu

Affiliation Department of Entomology and W. M. Keck Center for Behavioral Biology, North Carolina State University, Raleigh, North Carolina, United States of America
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NMR spectroscopy
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Centrifuges
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Contaminants
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Correlation spectroscopy
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Protons
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Centrifugation
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Hexanes
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Pipettes
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