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Ultralong C100 Mycolic Acids Support the Assignment of Segniliparus as a New Bacterial Genus

Figure 5

1H NMR analysis and structural summary of segnilomycolates.

(A) 1D TLC purified MAMEs were analyzed by 1H NMR. Spectral assignment for the chemical shifts and splitting patterns of mycolates were based on comparison with values reported in the literature. The large peak at 1.56 ppm was attributed to water and the singlet at 3.49 ppm was attributed to methanol in the samples. (B) Structural summary of Segniliparus mycolic acids. The number of carbons between the functional groups on the meromycolate chains were not determined here, but are based on approximate lengths previously reported.

Figure 5

doi: https://doi.org/10.1371/journal.pone.0039017.g005